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Presentation
Presentation
This curricular unit aims to understand the fundamentals associated with the chromatography and electroanalytical methods taught and the analytical possibilities that each of the techniques taught. It is also intended that students have the ability to independently perform the experimental procedures involving any of the analytical techniques taught and that are able, on the basis of acquired theoretical knowledge, to critically analyze experimental results and improve procedures.
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Class from course
Class from course
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Degree | Semesters | ECTS
Degree | Semesters | ECTS
Bachelor; Master Degree | Semestral | 6
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Year | Nature | Language
Year | Nature | Language
2 | Mandatory | Português
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Code
Code
ULHT477-3582
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Prerequisites and corequisites
Prerequisites and corequisites
Not applicable
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Professional Internship
Professional Internship
Não
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Syllabus
Syllabus
1. Chromatographic methods: a) Introduction and optimization of chromatographic separations. Fundamentals and applications: partition chromatography, planar chromatography, ion exchange chromatography and gel chromatography. b) Instrumentation and applications: Liquid Chromatography High Resolution, Gas Chromatography and Supercritical Fluid Chromatography. 2. Technical hyphenated: Concepts and applications. 3. Electroanalytical Methods: a) Conductometry: principles and instrumentation. b) Conductometric analysis methods: direct conductometry and conductometric titrations. c) Electrochemistry and introduction to electroanalytical methods. d) Potentiometry: introduction and instrumentation. Direct potentiometry and potentiometric titrations. e) Electroanalytical techniques: introduction to electrolysis. Fundamentals and applications: electrogravimetric analysis, coulometry, amperometry and voltammetry.
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Objectives
Objectives
The course of Analytical Methods II intends, to following the course of Analytical Methods I, and complement the knowledge already gained in this area with other equally important methods within the Pharmaceutical Sciences. Thus, analytical methods II will be addressed involving the methods of chromatographic separation, with particular relevance for liquid-liquid chromatography (HPLC), chromatography gas-liquid and, addressed last chromatography with supercritical fluids and hyphenated technics. Finally, we will study the electroanalytical methods: conductometric methods, potentiometry, electrogravimetry and coulometry.
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Teaching methodologies and assessment
Teaching methodologies and assessment
Throughout the teaching of the UC, practical and demonstrative examples of the matter are used.
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References
References
Harris, D.C. (2010). Quantitative Chemical Analysis. New York: W. H. Freeman & Co. ISBN-13: 978-1-4292-1815-3. Skoog, D., Holler, F. J., Crouch S. R. (2007). Principles of instrumental analysis. Belmont: Thomson Brooks/Cole. Skoog, D., Holler, F. J., Crouch S. R. (2013). Fundamentals of Analytical Chemistry, USA: Cengage Learning US. Christian, G.D. (2003). Analytical Chemistry. New York: John Wiley & Sons. Skoog, D., Holler, F. J., Crouch S. R. (2000). Analytical Chemistry: an Introduction. USA: Cengage Learning US.
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Office Hours
Office Hours
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Mobility
Mobility
No
